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食品研究与开发:2019,40(5):178-181
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氧弹燃烧-离子色谱法测定婴儿配方奶粉中的氯
(天津海关(原天津出入境检验检疫局)动植物与食品检测中心,天津300461)
Determination of Chlorine in Infant Formula Milk Powder by Ion Chromatography with Oxygen Bomb Combustion
(Animal&Plant and Food Inspection Center of Tianjin Customs(Former Tianjin Ispection and Quarantine Bureau),Tianjin 300461,China)
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投稿时间:2018-07-09    
中文摘要: 建立采用氧弹燃烧-离子色谱法测定婴儿配方奶粉中的氯含量的条件及方法。以氧弹对婴儿配方奶粉试样进行燃烧,10 mmol/L NaOH为吸收液进行吸收,以Dionex IonPac AS 11-HC柱,KOH梯度淋洗,流速为1.0 mL/min。经离子色谱分离测定婴儿配方奶粉中的氯的含量。氯离子的方法检出限为13.2 μg/L。利用该方法对婴儿配方奶粉中的氯进行测定,线性相关系数为0.999 9,平均回收率为91.0%~95.5%,相对标准偏差为1.9%~3.5%。
中文关键词: 氧弹燃烧  离子色谱  婴儿配方奶粉    测定
Abstract:The determination method of chlorine in infant formula milk powder by oxygen bomb comustion-ion chromatography and 10 mmol/L NaOH as the absorption solution was investigated.All species were separated at Dionex IonPac AS 11-HC column with mobile phase of KOH at a flow-rate of 1.0 mL/min.The detection limit of chloridion was 13.2 μg/L.The proposed method was used to determinate the chlorine in infant formula milk powder samples,the correlation coefficient was 0.999 9,the recoveries of the anions were in the range of 91.0%-95.5%,the relative standard deviations of chlorine were 1.9%-3.5%。
文章编号:201905032     中图分类号:    文献标志码:
基金项目:国家质量监督检验检疫总局科技计划项目(2016IK252)
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