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食品研究与开发:2025,46(16):169-174
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蓝莓皮花青素的产业化生产工艺优化和设计
(1.烟台职业学院 学生处,山东 烟台 264670;2.烟台大学 生命科学学院,山东 烟台 264006)
Industrial Production Process Optimization and Design of Blueberry Peel Anthocyanin
(1. Students′ Affairs Office,Yantai Vocational College,Yantai 264670,Shandong,China;2. School of Life Sciences,Yantai University,Yantai 264006,Shandong,China)
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投稿时间:2025-01-14    
中文摘要: 为探究蓝莓皮渣中花青素的开发利用价值,研究提取剂种类和体积分数、料液比、提取次数、提取时间对提取液花青素浓度的影响;并利用8种大孔树脂(X-5、XAD-16、DM-21、SP-207、LS-305、LS-610B、AB-8、D101)对提取液进行吸附纯化研究比较。结果表明,最佳提取剂为60%乙醇水溶液,最优提取条件为料液比1∶4 (g/mL),逆流提取3次,每次提取4 h。树脂纯化的结果表明,吸附和解吸性能最优树脂为LS-305。相比吸附前,树脂吸附纯化后得到的固体色素产品色价提高了3.1倍,花青素含量提高了4.6倍,收率降低了4.5倍。可针对产品色价的不同要求,设计不同的工艺流程,如要求色价18以下的产品,采用乙醇提取浓缩烘干工艺即可;若要求高色价的产品,需要采用吸附柱进行纯化。
中文关键词: 蓝莓皮  花青素  提取  大孔树脂  吸附  优化  设计
Abstract:To explore the development and utilization value of anthocyanins in blueberry peel residues,the effects of extraction agent type and volume fraction,solid-liquid ratio,extraction frequency,and extraction time on the concentration of anthocyanins in the extraction solution were studied. Eight types of macroporous resins(X-5,XAD-16,DM-21,SP-207,LS-305,LS-610B,AB-8,and D101) were used to compare the adsorption and purification of the extraction solution. The results showed that the optimal extraction agent was a 60% ethanol aqueous solution,and the optimal extraction conditions were as follows:a solid-liquid ratio of 1∶4(g/mL),countercurrent extraction for three times,and extraction for 4 h each time. The study on resin purification showed that LS-305 had the best adsorption and desorption performance. After adsorption,the color value of the solid pigment product obtained after resin adsorption and purification increased by 3.1 times;the anthocyanin content increased by 4.6 times,and the yield decreased by 4.5 times. According to the different requirements of customers for products′ color value,different process flows were designed. For those who required a color value below 18,ethanol extraction,concentration,and drying process could be used. If products with high color values were required,adsorption columns could be used for purification.
文章编号:202516022     中图分类号:    文献标志码:
基金项目:横向课题(SK19H21)
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